Titulo:

DEPOSITION AND PROPERTY CHARACTERISATION OF TaN COATINGS DEPOSITED WITH DIFFERENT NITROGEN CONTENTS
.

Sumario:

This work focused on the study of the influence of nitrogen content on the microstructure, chemical composition, mechanical and tribological properties of  TaN coatings deposited on 420 stainless steel and silicon samples (100) using the  magnetron sputtering technique. For the deposition of the TaN coatings an argon/nitrogen atmosphere was used, varying the flux of nitrogen between 12% and 25%. For coating’s characterization, Scanning electron microscopy, Energy dispersive X-ray spectroscopy, Atomic force microscopy, X-Ray diffraction, Microraman spectroscopy, Micro-hardness tester and a ball on disc tribometer were used. A refining of the columnar structure of the coatings, accompanied by a decrease in their thickness with the increased n... Ver más

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1794-1237

2463-0950

13

2016-10-25

69

80

Revista EIA/ English version - 2016

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spelling DEPOSITION AND PROPERTY CHARACTERISATION OF TaN COATINGS DEPOSITED WITH DIFFERENT NITROGEN CONTENTS
DEPOSITION AND PROPERTY CHARACTERISATION OF TaN COATINGS DEPOSITED WITH DIFFERENT NITROGEN CONTENTS
This work focused on the study of the influence of nitrogen content on the microstructure, chemical composition, mechanical and tribological properties of  TaN coatings deposited on 420 stainless steel and silicon samples (100) using the  magnetron sputtering technique. For the deposition of the TaN coatings an argon/nitrogen atmosphere was used, varying the flux of nitrogen between 12% and 25%. For coating’s characterization, Scanning electron microscopy, Energy dispersive X-ray spectroscopy, Atomic force microscopy, X-Ray diffraction, Microraman spectroscopy, Micro-hardness tester and a ball on disc tribometer were used. A refining of the columnar structure of the coatings, accompanied by a decrease in their thickness with the increased nitrogen content was observed. Initially, fcc-TaN (111) cubic phase growth was observed, this phase was changed to the fcc-TaN (200) above N2 12%. For contents greater than N2 18%, another nitrogen-rich phase was formed and the system tended to amorphicity, particularly for coating with N2 25% content. TaN-1 sample deposited with N2 12% in the gas mixture presented the highest micro-hardness value of 21.3GPa and the lowest friction coefficient and wear rate of 0.02 and 1.82x10-7 (mm3/Nm), respectively. From the obtained results, an important relationship between the microstructural, mechanical and tribological properties of the coated samples and their nitrogen content was observed.
Bejarano Gaitán, Gilberto
Echavarría García, Aida Milena
Quirama Ossa, Alix Caterine
Osorio Vélez, Jaime Alberto
Hard coatings
Magnetron sputtering
Tantalum nitride
Surface modification
Wear resistance
Tribology
13
25
Artículo de revista
Journal article
2016-10-25 00:00:00
2016-10-25 00:00:00
2016-10-25
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Revista EIA / English version
Revista EIA / English version
1794-1237
2463-0950
https://revistas.eia.edu.co/index.php/Reveiaenglish/article/view/1047
https://revistas.eia.edu.co/index.php/Reveiaenglish/article/view/1047
spa
https://creativecommons.org/licenses/by-nc-sa/4.0/
Revista EIA/ English version - 2016
69
80
https://revistas.eia.edu.co/index.php/Reveiaenglish/article/download/1047/1019
info:eu-repo/semantics/article
http://purl.org/coar/resource_type/c_6501
http://purl.org/redcol/resource_type/ARTREF
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/version/c_970fb48d4fbd8a85
info:eu-repo/semantics/openAccess
http://purl.org/coar/access_right/c_abf2
Text
Publication
institution UNIVERSIDAD EIA
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collection Revista EIA / English version
title DEPOSITION AND PROPERTY CHARACTERISATION OF TaN COATINGS DEPOSITED WITH DIFFERENT NITROGEN CONTENTS
spellingShingle DEPOSITION AND PROPERTY CHARACTERISATION OF TaN COATINGS DEPOSITED WITH DIFFERENT NITROGEN CONTENTS
Bejarano Gaitán, Gilberto
Echavarría García, Aida Milena
Quirama Ossa, Alix Caterine
Osorio Vélez, Jaime Alberto
Hard coatings
Magnetron sputtering
Tantalum nitride
Surface modification
Wear resistance
Tribology
title_short DEPOSITION AND PROPERTY CHARACTERISATION OF TaN COATINGS DEPOSITED WITH DIFFERENT NITROGEN CONTENTS
title_full DEPOSITION AND PROPERTY CHARACTERISATION OF TaN COATINGS DEPOSITED WITH DIFFERENT NITROGEN CONTENTS
title_fullStr DEPOSITION AND PROPERTY CHARACTERISATION OF TaN COATINGS DEPOSITED WITH DIFFERENT NITROGEN CONTENTS
title_full_unstemmed DEPOSITION AND PROPERTY CHARACTERISATION OF TaN COATINGS DEPOSITED WITH DIFFERENT NITROGEN CONTENTS
title_sort deposition and property characterisation of tan coatings deposited with different nitrogen contents
description This work focused on the study of the influence of nitrogen content on the microstructure, chemical composition, mechanical and tribological properties of  TaN coatings deposited on 420 stainless steel and silicon samples (100) using the  magnetron sputtering technique. For the deposition of the TaN coatings an argon/nitrogen atmosphere was used, varying the flux of nitrogen between 12% and 25%. For coating’s characterization, Scanning electron microscopy, Energy dispersive X-ray spectroscopy, Atomic force microscopy, X-Ray diffraction, Microraman spectroscopy, Micro-hardness tester and a ball on disc tribometer were used. A refining of the columnar structure of the coatings, accompanied by a decrease in their thickness with the increased nitrogen content was observed. Initially, fcc-TaN (111) cubic phase growth was observed, this phase was changed to the fcc-TaN (200) above N2 12%. For contents greater than N2 18%, another nitrogen-rich phase was formed and the system tended to amorphicity, particularly for coating with N2 25% content. TaN-1 sample deposited with N2 12% in the gas mixture presented the highest micro-hardness value of 21.3GPa and the lowest friction coefficient and wear rate of 0.02 and 1.82x10-7 (mm3/Nm), respectively. From the obtained results, an important relationship between the microstructural, mechanical and tribological properties of the coated samples and their nitrogen content was observed.
author Bejarano Gaitán, Gilberto
Echavarría García, Aida Milena
Quirama Ossa, Alix Caterine
Osorio Vélez, Jaime Alberto
author_facet Bejarano Gaitán, Gilberto
Echavarría García, Aida Milena
Quirama Ossa, Alix Caterine
Osorio Vélez, Jaime Alberto
topicspa_str_mv Hard coatings
Magnetron sputtering
Tantalum nitride
Surface modification
Wear resistance
Tribology
topic Hard coatings
Magnetron sputtering
Tantalum nitride
Surface modification
Wear resistance
Tribology
topic_facet Hard coatings
Magnetron sputtering
Tantalum nitride
Surface modification
Wear resistance
Tribology
citationvolume 13
citationissue 25
publisher Revista EIA / English version
ispartofjournal Revista EIA / English version
source https://revistas.eia.edu.co/index.php/Reveiaenglish/article/view/1047
language spa
format Article
rights https://creativecommons.org/licenses/by-nc-sa/4.0/
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publishDate 2016-10-25
date_accessioned 2016-10-25 00:00:00
date_available 2016-10-25 00:00:00
url https://revistas.eia.edu.co/index.php/Reveiaenglish/article/view/1047
url_doi https://revistas.eia.edu.co/index.php/Reveiaenglish/article/view/1047
issn 1794-1237
eissn 2463-0950
citationstartpage 69
citationendpage 80
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